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A reversed-phase HPLC chromatogram with a shallow enough gradient to resolve deamidation and truncation impurities, an LC-MS spectrum matching 1,419.5 Da, endotoxin by kinetic chromogenic LAL, residual solvents by GC, and Karl Fischer water content

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The spontaneously diabetic biobreeding (BB) rat model of T1D shows an increased amount of permeability in the stomach, small intestine and the colon [169]