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The mobile phase consisted of solvent A (10 mM ammonium acetate with 1% acetic acid in water) and solvent B (acetonitrile) delivered at a flow rate of 0.35 mL/min with a linear gradient as follows: 25% B until 3 min, 25–40% B over 3.9 min, 40–70% B from 3.9 to 4 min, decreased to 25% B from 4 to 4.6 min, and maintained at 25% B until 5.5 min

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